Molybdenum-Enhanced Conductivity and Nickel Electron Density Synergizing With Phosphorus-Induced Oxygen Vacancies in NiMo-Based Heterostructures for Efficient Electrooxidation of 5-Hydroxymethylfurfural.
5-Hydroxymethylfurfural (HMF) can be electrocatalytically oxidized to 2,5-furandicarboxylic acid (FDCA) with concurrent hydrogen evolution, providing a sustainable route for biomass valorization and clean energy generation. In this study, we synthesized a three-dimensional nanorod heterostructured catalyst composed of...