Author

A. Samala

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Open access Aug 2026

AQbD-Guided Stability-Indicating UHPLC Method for Simultaneous Determination of Major Withanolides in Ashwagandha Root Extract and Commercial Capsules

A rapid, stability-indicating, and environmentally considerate ultra-high-performance liquid chromatographic (UHPLC) method was developed for simultaneous determination of withanoside IV, withanoside V, withaferin A, 12-deoxywithastramonolide, withanolide A, and withanolide B in Ashwagandha root extract and commercial...

G. Kiran, A. Samala, N. Raghunandan et al. · IJPAR JOURNAL · 0 citations

Open access Aug 2026

AQbD-Optimised Stability-Indicating Green RP-HPLC Method for Simultaneous Determination of Adapalene and Benzoyl Peroxide in Topical Gel

A tetrahydrofuran-free, stability-indicating reversed-phase HPLC method was developed for simultaneous determination of adapalene and benzoyl peroxide in a commercial topical gel. Analytical Quality by Design (AQbD) was used to define the analytical target profile, identify high-risk chromatographic variables, and eval...

A. Samala, G. Kiran, N. Raghunandan et al. · IJPAR JOURNAL · 0 citations

Open access Aug 2026

AQbD-Guided Stability-Indicating RP-HPLC-DAD Method for Curcuminoids in Commercial Capsules with Targeted Dye-Adulterant Screening

A stability-indicating reversed-phase HPLC method with diode-array detection was developed for simultaneous determination of curcumin, demethoxycurcumin, and bisdemethoxycurcumin in commercial capsules, with targeted screening for metanil yellow and Sudan I. Analytical Quality by Design was applied through definition o...

Vattem Supriya, A. Samala, Gadipally Sai Kiran et al. · IJPAR JOURNAL · 0 citations